Epiperchloratohydrin (I) was synthesized and polymerized; although covalent perchlorates are known to be hydrolytically unstable. Compound (I), dissolved in benzene could be rapidly washed with water without causing major hydrolysis. A simple method for dehydrating silver perchlorate by an azeotropic distillation was used. Compound (I) before and after polymerization was explosive and required special care.
"Epiperchloratohydrin (I) was synthesized and polymerized; although covalent perchlorates are known to be hydrolytically unstable. Compound (I), dissolved in benzene could be rapidly washed with water without causing major hydrolysis. A simple method for dehydrating silver perchlorate by an azeotropic distillation was used. Compound (I) before and after polymerization was explosive and required special care."@en
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